Development and Characterization of Novel Complex Hydrides Synthesized via Molten State Processing

Development of Novel Polymer Nanostructures and Nanoscale Complex Hydrides for Reversible Hydrogen Storage

On the Reversibility of Hydrogen Storage in Novel Complex Hydrides

A comparison of the hydrogen release and uptake (cycling) capability of Ti-doped NaAlH4, LiAlH4 and Mg(AlH4)2 as a function of Ti dopant concentration, temperature, pressure, and cycle number is reported. Temperature programmed desorption revealed hydrogen release capacities of around 3 wt% at 140 C, 3 wt % at 100 C and 6 wt% at 150 C, respectively for the Ti doped Na, Li and Mg alanates. In th...

synthesis and characterization of some macrocyclic schiff bases

ماکروسیکلهای شیف باز از اهمیت زیادی در شیمی آلی و دارویی برخوردار می باشند. این ماکروسیکلها با دارابودن گروه های مناسب در مکانهای مناسب می توانند فلزاتی مثل مس، نیکل و ... را در حفره های خود به دام انداخته، کمپلکسهای پایدار تولید نمایند. در این پایان نامه ابتدا یک دی آلدئید آروماتیک از گلیسیرین تهیه می شود و در مرحله بعدی واکنش با دی آمینهای آروماتیک و یا آلیفاتیک در رقتهای بسیار زیاد منجر به ت...

Synthesis and Characterization of Nano-Size CaCO3 via Thermal Treatment and Solid State Method.

CaCO3 nanoparticles have been synthesized via heat-treatment of a new precursor and solid state reaction. Effect of calcinations temperature and quantity of surfactant on particle size has been investigated. The products were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and Fourier transform infrared (FT–IR) spec...

On the fabrication and characterization of Al5083/Al2O3 surface nanocomposite via friction stir processing

In the present study, Al5083- Al2O3 nanocomposite was successfully prepared by friction stir processing (FSP) with rotational speed of 710 rpm and travel speed of 14 mm/min. In order to improve distribution of Al2O3 particles, a net of holes were designed on the surface of Al5083 sheet. The samples were characterized by optical and scanning electron microscopy (SEM), microhardness, tensile and ...